Information card for entry 4314685

Structure parameters

• Formula: C54 H72 B3 F24 N2 P2 Rh
• Calculated formula: C54 H72 B3 F24 N2 P2 Rh
• Title of publication: Amine- and Dimeric Amino-Borane Complexes of the {Rh(PiPr3)2}+ Fragment and Their Relevance to the Transition-Metal-Mediated Dehydrocoupling of Amine-Boranes
• Authors of publication: Adrian B. Chaplin; Andrew S. Weller
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 1111 - 1121
• a: 13.6939 ± 0.0007 Å
• b: 13.6939 ± 0.0007 Å
• c: 34.408 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6452.3 ± 0.7 ų
• Cell temperature: 220 ± 2 K
• Ambient diffraction temperature: 220 ± 2 K
• Number of distinct elements: 7
• Space group number: 92
• Hermann-Mauguin space group symbol: P 41 21 2
• Hall space group symbol: P 4abw 2nw
• Residual factor for all reflections: 0.0978
• Residual factor for significantly intense reflections: 0.0692
• Weighted residual factors for significantly intense reflections: 0.1507
• Weighted residual factors for all reflections included in the refinement: 0.1702
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No