Information card for entry 4315381

Structure parameters

• Formula: C22 H56 F6 P7 Re
• Calculated formula: C22 H56 F6 P7 Re
• Title of publication: Luminescent Low-Valent Rhenium Complexes with 1,2-Bis(dialkylphosphino)ethane Ligands. Synthesis and X-ray Crystallographic, Electrochemical, and Spectroscopic Characterization
• Authors of publication: Stephania J. Messersmith; Kristin Kirschbaum; Jon R. Kirchhoff
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 3857 - 3865
• a: 10.2719 ± 0.001 Å
• b: 21.078 ± 0.002 Å
• c: 15.7963 ± 0.0016 Å
• α: 90°
• β: 100.194 ± 0.002°
• γ: 90°
• Cell volume: 3366.1 ± 0.6 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0458
• Residual factor for significantly intense reflections: 0.0334
• Weighted residual factors for significantly intense reflections: 0.0831
• Weighted residual factors for all reflections included in the refinement: 0.0895
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No