Crystallography Open Database

Information card for entry 4315382

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Coordinates	4315382.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H59 F12 N P8 Re
Calculated formula	C24 H59 F12 N P8 Re
Title of publication	Luminescent Low-Valent Rhenium Complexes with 1,2-Bis(dialkylphosphino)ethane Ligands. Synthesis and X-ray Crystallographic, Electrochemical, and Spectroscopic Characterization
Authors of publication	Stephania J. Messersmith; Kristin Kirschbaum; Jon R. Kirchhoff
Journal of publication	Inorganic Chemistry
Year of publication	2010
Journal volume	49
Pages of publication	3857 - 3865
a	10.8891 ± 0.0009 Å
b	11.3233 ± 0.0009 Å
c	19.4 ± 0.003 Å
α	73.211 ± 0.007°
β	79.304 ± 0.007°
γ	64.972 ± 0.003°
Cell volume	2069.5 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1001
Residual factor for significantly intense reflections	0.0559
Weighted residual factors for significantly intense reflections	0.1216
Weighted residual factors for all reflections included in the refinement	0.1384
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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