Information card for entry 4315527

Structure parameters

• Formula: C44 H94 K2 N6 P2 Si4
• Calculated formula: C44 H94 K2 N6 P2 Si4
• Title of publication: Germanium(II) and Tin(II) Complexes of a Sterically Demanding Phosphanide Ligand
• Authors of publication: Keith Izod; John Stewart; Ewan R. Clark; William Clegg; Ross W. Harrington
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 4698 - 4707
• a: 13.538 ± 0.003 Å
• b: 13.331 ± 0.003 Å
• c: 17.801 ± 0.003 Å
• α: 90°
• β: 111.225 ± 0.014°
• γ: 90°
• Cell volume: 2994.7 ± 1.1 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1027
• Residual factor for significantly intense reflections: 0.0579
• Weighted residual factors for significantly intense reflections: 0.1142
• Weighted residual factors for all reflections included in the refinement: 0.1291
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No