Information card for entry 4315529

Structure parameters

• Formula: C55 H104 Li O4 P3 Si6 Sn
• Calculated formula: C54.96 H103.92 Li O4 P3 Si6 Sn
• Title of publication: Germanium(II) and Tin(II) Complexes of a Sterically Demanding Phosphanide Ligand
• Authors of publication: Keith Izod; John Stewart; Ewan R. Clark; William Clegg; Ross W. Harrington
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 4698 - 4707
• a: 39.504 ± 0.01 Å
• b: 39.504 ± 0.01 Å
• c: 39.504 ± 0.01 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 61649 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 219
• Hermann-Mauguin space group symbol: F -4 3 c
• Hall space group symbol: F -4a 2 3
• Residual factor for all reflections: 0.1108
• Residual factor for significantly intense reflections: 0.0552
• Weighted residual factors for significantly intense reflections: 0.1137
• Weighted residual factors for all reflections included in the refinement: 0.1456
• Goodness-of-fit parameter for all reflections included in the refinement: 1.109
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No