Information card for entry 4316683

Structure parameters

• Formula: C33 H43 Cl3 O Os P2
• Calculated formula: C33 H43 Cl3 O Os P2
• Title of publication: Osmium(III) Complexes with POP Pincer Ligands: Preparation from Commercially Available OsCl3.3H2O and Their X-ray Structures
• Authors of publication: Gregorio Asensio; Ana B. Cuenca; Miguel A. Esteruelas; Mercedes Medio-Simón; Montserrat Oliván; Marta Valencia
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 8665 - 8667
• a: 9.171 ± 0.002 Å
• b: 14.545 ± 0.004 Å
• c: 24.413 ± 0.006 Å
• α: 90°
• β: 94.56 ± 0.004°
• γ: 90°
• Cell volume: 3246.2 ± 1.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0348
• Residual factor for significantly intense reflections: 0.0262
• Weighted residual factors for significantly intense reflections: 0.0504
• Weighted residual factors for all reflections included in the refinement: 0.052
• Goodness-of-fit parameter for all reflections included in the refinement: 0.959
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No