Information card for entry 4316684

Structure parameters

• Formula: C27 H40 Cl3 O Os P2
• Calculated formula: C27 H40 Cl3 O Os P2
• SMILES: [Os]12(Cl)(Cl)(Cl)[P](C(C)C)(C(C)C)c3cccc4c3[O]2c2c(C4(C)C)cccc2[P]1(C(C)C)C(C)C
• Title of publication: Osmium(III) Complexes with POP Pincer Ligands: Preparation from Commercially Available OsCl3.3H2O and Their X-ray Structures
• Authors of publication: Gregorio Asensio; Ana B. Cuenca; Miguel A. Esteruelas; Mercedes Medio-Simón; Montserrat Oliván; Marta Valencia
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 8665 - 8667
• a: 21.643 ± 0.007 Å
• b: 17.961 ± 0.006 Å
• c: 15.261 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5932 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.0567
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for significantly intense reflections: 0.0403
• Weighted residual factors for all reflections included in the refinement: 0.0432
• Goodness-of-fit parameter for all reflections included in the refinement: 0.696
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No