Information card for entry 4317514

Structure parameters

• Formula: C82 H80 N14 Sm4 Te11
• Calculated formula: C82 H80 N14 Sm4 Te11
• Title of publication: Chalcogen-Rich Lanthanide Clusters: Compounds with Te2-, (TeTe)2-, TePh, TeTePh, (TeTeTe(Ph)TeTe)5-, and [(TeTe)4TePh]9- Ligands; Single Source Precursors to Solid-State Lanthanide Tellurides
• Authors of publication: Deborah Freedman; Thomas J. Emge; John G. Brennan
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 492 - 500
• a: 12.191 ± 0.005 Å
• b: 27.484 ± 0.005 Å
• c: 28.484 ± 0.005 Å
• α: 90 ± 0.02°
• β: 91.56 ± 0.02°
• γ: 90 ± 0.02°
• Cell volume: 9540 ± 5 ų
• Cell temperature: 123 ± 5 K
• Ambient diffraction temperature: 123 ± 5 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1335
• Residual factor for significantly intense reflections: 0.0661
• Weighted residual factors for significantly intense reflections: 0.1516
• Weighted residual factors for all reflections included in the refinement: 0.165
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No