Information card for entry 4317515

Structure parameters

• Formula: C64.5 H62.5 N10.5 Tb4 Te11.07
• Calculated formula: C64.5 H62.5 N10.5 Tb4 Te11.073
• Title of publication: Chalcogen-Rich Lanthanide Clusters: Compounds with Te2-, (TeTe)2-, TePh, TeTePh, (TeTeTe(Ph)TeTe)5-, and [(TeTe)4TePh]9- Ligands; Single Source Precursors to Solid-State Lanthanide Tellurides
• Authors of publication: Deborah Freedman; Thomas J. Emge; John G. Brennan
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 492 - 500
• a: 12.85 ± 0.025 Å
• b: 31.13 ± 0.015 Å
• c: 20.37 ± 0.005 Å
• α: 90 ± 0.03°
• β: 91.5 ± 0.05°
• γ: 90 ± 0.12°
• Cell volume: 8146 ± 16 ų
• Cell temperature: 153 ± 5 K
• Ambient diffraction temperature: 153 ± 5 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.155
• Residual factor for significantly intense reflections: 0.0673
• Weighted residual factors for significantly intense reflections: 0.1488
• Weighted residual factors for all reflections included in the refinement: 0.1666
• Goodness-of-fit parameter for all reflections included in the refinement: 1.008
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No