Information card for entry 4317516

Structure parameters

• Formula: C62 H60 N10 Te11.57 Tm4
• Calculated formula: C62 H60 N10 Te11.57 Tm4
• Title of publication: Chalcogen-Rich Lanthanide Clusters: Compounds with Te2-, (TeTe)2-, TePh, TeTePh, (TeTeTe(Ph)TeTe)5-, and [(TeTe)4TePh]9- Ligands; Single Source Precursors to Solid-State Lanthanide Tellurides
• Authors of publication: Deborah Freedman; Thomas J. Emge; John G. Brennan
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 492 - 500
• a: 23.407 ± 0.007 Å
• b: 23.2 ± 0.02 Å
• c: 17.507 ± 0.009 Å
• α: 90 ± 0.06°
• β: 113.38 ± 0.04°
• γ: 90 ± 0.04°
• Cell volume: 8726 ± 10 ų
• Cell temperature: 153 ± 5 K
• Ambient diffraction temperature: 153 ± 5 K
• Number of distinct elements: 5
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.1569
• Residual factor for significantly intense reflections: 0.0877
• Weighted residual factors for significantly intense reflections: 0.2149
• Weighted residual factors for all reflections included in the refinement: 0.2403
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No