Information card for entry 4317519

Structure parameters

• Formula: C42 H60 Al Cl4 N2 O4 P
• Calculated formula: C42 H60 Al Cl4 N2 O4 P
• Title of publication: Ligand-Tetrahydrofuran Coupling in Chelated Aluminum Phosphinates
• Authors of publication: Y. Wang; S. Parkin; D. Atwood
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 558 - 565
• a: 12.101 ± 0.002 Å
• b: 12.533 ± 0.002 Å
• c: 16.136 ± 0.002 Å
• α: 91.552 ± 0.01°
• β: 106.656 ± 0.01°
• γ: 104.09 ± 0.01°
• Cell volume: 2261.6 ± 0.6 ų
• Cell temperature: 173 ± 1 K
• Ambient diffraction temperature: 173 ± 1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.07
• Residual factor for significantly intense reflections: 0.0507
• Weighted residual factors for significantly intense reflections: 0.1179
• Weighted residual factors for all reflections included in the refinement: 0.1257
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No