Information card for entry 4317520

Structure parameters

• Formula: C53 H64 Al N2 O3 P
• Calculated formula: C47 H64 Al N2 O4 P
• Title of publication: Ligand-Tetrahydrofuran Coupling in Chelated Aluminum Phosphinates
• Authors of publication: Y. Wang; S. Parkin; D. Atwood
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 558 - 565
• a: 12.142 ± 0.005 Å
• b: 12.876 ± 0.005 Å
• c: 15.904 ± 0.005 Å
• α: 92.15 ± 0.02°
• β: 107.82 ± 0.02°
• γ: 107.11 ± 0.02°
• Cell volume: 2240 ± 1.5 ų
• Cell temperature: 173 ± 1 K
• Ambient diffraction temperature: 173 ± 1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1357
• Residual factor for significantly intense reflections: 0.0888
• Weighted residual factors for significantly intense reflections: 0.1187
• Weighted residual factors for all reflections included in the refinement: 0.1292
• Goodness-of-fit parameter for all reflections included in the refinement: 1.156
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No