Information card for entry 4317533

Structure parameters

• Common name: (SnPh2Cl2).H2O/[SnPh2Cl2.VO(3-MeOsalen)]
• Chemical name: [Diphenyltin dichloride.aqua(1/1)/{diphenyltin dichloride.[N,N'-bis(3-methoxysalicylidene)ethane-1,2-diaminato]oxovan adium(IV)(1/1)}](1/1)
• Formula: C44 H42 Cl8 N2 O6 Sn2 V
• Calculated formula: C44 H42 Cl8 N2 O6 Sn2 V
• Title of publication: Donor Properties of the Vanadyl Ion: Reactions of Vanadyl Salicylaldimine β-Ketimine and Acetylacetonato Complexes with Groups 14 and 15 Lewis Acids
• Authors of publication: B. Cashin; D. Cunningham; P. Daly; P. McArdle; M. Munroe; N. Ní Chonchubhair
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 773 - 782
• a: 12.959 ± 0.003 Å
• b: 15.783 ± 0.004 Å
• c: 24.795 ± 0.007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5071 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0492
• Residual factor for significantly intense reflections: 0.0385
• Weighted residual factors for significantly intense reflections: 0.1189
• Weighted residual factors for all reflections included in the refinement: 0.1252
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No