Information card for entry 4317534

Structure parameters

• Common name: SnPh2Cl2.VO(acetophen1,2pn)
• Chemical name: Diphenyltin dichloride.[N,N'-bis(alpha-methylsalicylidene)ethane-1,2-diaminato]oxo vanadium(IV) (1/1)
• Formula: C32 H32 Cl4 N2 O3 Sn V
• Calculated formula: C32 H32 Cl4 N2 O3 Sn V
• Title of publication: Donor Properties of the Vanadyl Ion: Reactions of Vanadyl Salicylaldimine β-Ketimine and Acetylacetonato Complexes with Groups 14 and 15 Lewis Acids
• Authors of publication: B. Cashin; D. Cunningham; P. Daly; P. McArdle; M. Munroe; N. Ní Chonchubhair
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 773 - 782
• a: 11.184 ± 0.004 Å
• b: 17.181 ± 0.003 Å
• c: 17.528 ± 0.002 Å
• α: 89.988 ± 0.013°
• β: 92.178 ± 0.018°
• γ: 90.006 ± 0.019°
• Cell volume: 3365.6 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.143
• Residual factor for significantly intense reflections: 0.0966
• Weighted residual factors for significantly intense reflections: 0.2356
• Weighted residual factors for all reflections included in the refinement: 0.2628
• Goodness-of-fit parameter for all reflections included in the refinement: 0.968
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No