Information card for entry 4318223

Structure parameters

• Formula: C44 H24 O19 Os6 P4
• Calculated formula: C44 H22 O19 Os6 P4
• SMILES: [Os]1([Os]([Os]1(C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C#[O])(C#[O])C#[O])([P]1([P]2([Os]3([Os]([Os]3(C#[O])(C#[O])(C#[O])C#[O])([P](P2c2ccccc2)(C1)c1ccccc1)(C#[O])C#[O])(C#[O])C#[O])c1ccccc1)c1ccccc1)(C#[O])(C#[O])C#[O]
• Title of publication: 1,2,3,4-Tetraphenyl-1,2,3,4-tetraphospholane, a Highly Versatile Cyclocarbaphosphine Ligand: Reactions with Activated Triosmium Clusters and Characterization of the Products
• Authors of publication: Siau-Gek Ang; Zhong; How-Ghee Ang
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 3791 - 3800
• a: 12.1994 ± 0.0007 Å
• b: 22.5939 ± 0.0013 Å
• c: 18.7303 ± 0.0011 Å
• α: 90°
• β: 94.799 ± 0.001°
• γ: 90°
• Cell volume: 5144.6 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0509
• Residual factor for significantly intense reflections: 0.036
• Weighted residual factors for significantly intense reflections: 0.0697
• Weighted residual factors for all reflections included in the refinement: 0.0725
• Goodness-of-fit parameter for all reflections included in the refinement: 0.923
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No