Information card for entry 4318224

Structure parameters

• Formula: C41.5 H26.5 Cl1.5 O16 Os6 P4
• Calculated formula: C21 H11.5 Cl1.5 O8 Os3 P2
• Title of publication: 1,2,3,4-Tetraphenyl-1,2,3,4-tetraphospholane, a Highly Versatile Cyclocarbaphosphine Ligand: Reactions with Activated Triosmium Clusters and Characterization of the Products
• Authors of publication: Siau-Gek Ang; Zhong; How-Ghee Ang
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 3791 - 3800
• a: 23.0038 ± 0.0003 Å
• b: 13.508 ± 0.0002 Å
• c: 21.687 ± 0.0001 Å
• α: 90°
• β: 118.32°
• γ: 90°
• Cell volume: 5932.35 ± 0.12 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0766
• Residual factor for significantly intense reflections: 0.0501
• Weighted residual factors for significantly intense reflections: 0.1033
• Weighted residual factors for all reflections included in the refinement: 0.118
• Goodness-of-fit parameter for all reflections included in the refinement: 1.164
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No