Information card for entry 4318303

Structure parameters

• Formula: C44 H72 B5 O6 P4 Rh
• Calculated formula: C41 H74 B3.5 O4 P3 Rh0.5
• Title of publication: Tetraarylpentaborates, [B5O6Ar4]- (Ar = C6H4OMe-4, C6H3Me2-2,6): Their Formation from the Reaction of Arylboronic Acids with an Aryloxorhodium Complex, Structure, and Chemical Properties
• Authors of publication: Yasushi Nishihara; Kyoko Nara; Kohtaro Osakada
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 4090 - 4092
• a: 23.704 ± 0.006 Å
• b: 17.254 ± 0.008 Å
• c: 13.304 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5441 ± 3 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0565
• Residual factor for significantly intense reflections: 0.056
• Weighted residual factors for all reflections: 0.05
• Weighted residual factors for all reflections included in the refinement: 0.05
• Goodness-of-fit parameter for all reflections: 3.639
• Goodness-of-fit parameter for all reflections included in the refinement: 3.64
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoK?a
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No