Information card for entry 4318304

Structure parameters

• Formula: C40 H64 B5 O10 P4 Rh
• Calculated formula: C40 H64 B5 O10 P4 Rh
• SMILES: [Rh]([P](C)(C)C)([P](C)(C)C)([P](C)(C)C)[P](C)(C)C.O1[B]2(OB(OB1c1ccc(OC)cc1)c1ccc(OC)cc1)OB(OB(O2)c1ccc(OC)cc1)c1ccc(OC)cc1
• Title of publication: Tetraarylpentaborates, [B5O6Ar4]- (Ar = C6H4OMe-4, C6H3Me2-2,6): Their Formation from the Reaction of Arylboronic Acids with an Aryloxorhodium Complex, Structure, and Chemical Properties
• Authors of publication: Yasushi Nishihara; Kyoko Nara; Kohtaro Osakada
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 4090 - 4092
• a: 14.76 ± 0.0005 Å
• b: 17.1675 ± 0.0005 Å
• c: 19.8654 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5033.7 ± 0.3 ų
• Cell temperature: 213.2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for significantly intense reflections: 0.0559
• Weighted residual factors for all reflections included in the refinement: 0.0753
• Goodness-of-fit parameter for all reflections included in the refinement: 1.691
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoK?a
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No