Information card for entry 4318793

Structure parameters

• Formula: C10 H10.67 N2 O12.33 P2 V3
• Calculated formula: C10 H8 N2 O12.3333 P2 V3
• Title of publication: Novel Oxovanadium Phosphate Tubule Incorporating 2,2-Bipyridine Ligands: Hydrothermal Synthesis and Crystal Structure of [(VIVO)3(μ5-PO4)2(2,2'-bpy)(μ-OH2)].1/3H2O
• Authors of publication: Wenbin Yang; Canzhong Lu
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 5638 - 5640
• a: 29.76 ± 0.0003 Å
• b: 29.76 ± 0.0003 Å
• c: 9.5745 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 7343.66 ± 0.19 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0497
• Residual factor for significantly intense reflections: 0.037
• Weighted residual factors for significantly intense reflections: 0.0976
• Weighted residual factors for all reflections included in the refinement: 0.1151
• Goodness-of-fit parameter for all reflections included in the refinement: 1.148
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No