Information card for entry 4319240

Structure parameters

• Formula: C68.92 H152.46 N6.46 O62.54 S2 W18
• Calculated formula: C68.92 N6.46 O62.5648 S2.0008 W18.0072
• Title of publication: Synthesis and Redox Characterization of the Polyoxo Anion, γ*-[S2W18O62]4-: A Unique Fast Oxidation Pathway Determines the Characteristic Reversible Electrochemical Behavior of Polyoxometalate Anions in Acidic Media
• Authors of publication: Peter J. S. Richardt; Robert W. Gable; Alan M. Bond; Anthony G. Wedd
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 703 - 709
• a: 22.389 ± 0.006 Å
• b: 22.104 ± 0.003 Å
• c: 25.505 ± 0.005 Å
• α: 90°
• β: 95.69 ± 0.015°
• γ: 90°
• Cell volume: 12560 ± 5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1004
• Residual factor for significantly intense reflections: 0.0552
• Weighted residual factors for significantly intense reflections: 0.1356
• Weighted residual factors for all reflections included in the refinement: 0.1483
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No