Information card for entry 4319241

Structure parameters

• Formula: C15.5 H13 B Cu0.5 F9 K N6 O1.5
• Calculated formula: C15.5 H13 B Cu0.5 F9 K N6 O1.5
• Title of publication: Synthesis and Characterization of Fluorinated Tris(pyrazolyl)borate Complexes. Observation of an (η5-Pyrazole)-K+ Interaction in the Solid State
• Authors of publication: Zhengbo Hu; Sergiu M. Gorun
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 667 - 671
• a: 12.0411 ± 0.0002 Å
• b: 14.9791 ± 0.0002 Å
• c: 16.0567 ± 0.0003 Å
• α: 71.301 ± 0.001°
• β: 69.785 ± 0.001°
• γ: 66.539 ± 0.001°
• Cell volume: 2436.01 ± 0.07 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0792
• Residual factor for significantly intense reflections: 0.0461
• Weighted residual factors for all reflections: 0.1397
• Weighted residual factors for significantly intense reflections: 0.1149
• Goodness-of-fit parameter for all reflections: 1.05
• Goodness-of-fit parameter for significantly intense reflections: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No