Information card for entry 4320797

Structure parameters

• Formula: Cl4 Os2 Re4 Se8
• Calculated formula: Cl4 Os1.98 Re4.02 Se8
• Title of publication: Heterometal Substitution in the Dimensional Reduction of Cluster Frameworks: Synthesis of Soluble [Re6-nOsnSe8Cl6](4-n) (n = 1-3) Cluster-Containing Solids
• Authors of publication: Eric G. Tulsky; Jeffrey R. Long
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 6990 - 7002
• a: 8.7946 ± 0.0007 Å
• b: 8.8305 ± 0.0007 Å
• c: 11.9783 ± 0.0003 Å
• α: 87.818 ± 0.001°
• β: 84.896 ± 0.003°
• γ: 63.824 ± 0.004°
• Cell volume: 831.53 ± 0.1 ų
• Cell temperature: 155 ± 2 K
• Ambient diffraction temperature: 155 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0887
• Residual factor for significantly intense reflections: 0.0458
• Weighted residual factors for all reflections: 0.1046
• Weighted residual factors for significantly intense reflections: 0.0951
• Goodness-of-fit parameter for all reflections: 0.908
• Goodness-of-fit parameter for significantly intense reflections: 1.095
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No