Information card for entry 4320798

Structure parameters

• Formula: Cl6 Cs3 H4 O2 Os Re5 Se8
• Calculated formula: Cl6 Cs3 O2 Os1.02 Re4.98 Se8
• Title of publication: Heterometal Substitution in the Dimensional Reduction of Cluster Frameworks: Synthesis of Soluble [Re6-nOsnSe8Cl6](4-n) (n = 1-3) Cluster-Containing Solids
• Authors of publication: Eric G. Tulsky; Jeffrey R. Long
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 6990 - 7002
• a: 9.7255 ± 0.0007 Å
• b: 12.8958 ± 0.0009 Å
• c: 11.83 ± 0.0009 Å
• α: 90°
• β: 113.918 ± 0.001°
• γ: 90°
• Cell volume: 1356.29 ± 0.17 ų
• Cell temperature: 161 ± 2 K
• Ambient diffraction temperature: 161 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0684
• Residual factor for significantly intense reflections: 0.0589
• Weighted residual factors for all reflections: 0.1651
• Weighted residual factors for significantly intense reflections: 0.1606
• Goodness-of-fit parameter for all reflections: 1.053
• Goodness-of-fit parameter for significantly intense reflections: 1.142
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No