Information card for entry 4320801

Structure parameters

• Formula: C56 H128 Cl6 N3 O2 Os Re5 Se8
• Calculated formula: C54.5 H58 Cl6 N2 O Os1.02 Re4.98 Se8
• Title of publication: Heterometal Substitution in the Dimensional Reduction of Cluster Frameworks: Synthesis of Soluble [Re6-nOsnSe8Cl6](4-n) (n = 1-3) Cluster-Containing Solids
• Authors of publication: Eric G. Tulsky; Jeffrey R. Long
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 6990 - 7002
• a: 12.5328 ± 0.0004 Å
• b: 12.5489 ± 0.0005 Å
• c: 13.9561 ± 0.0005 Å
• α: 85.714 ± 0.001°
• β: 76.901 ± 0.001°
• γ: 72.122 ± 0.001°
• Cell volume: 2034.54 ± 0.13 ų
• Cell temperature: 161 ± 2 K
• Ambient diffraction temperature: 161 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.097
• Residual factor for significantly intense reflections: 0.053
• Weighted residual factors for all reflections: 0.1383
• Weighted residual factors for significantly intense reflections: 0.124
• Goodness-of-fit parameter for all reflections: 0.854
• Goodness-of-fit parameter for significantly intense reflections: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No