Information card for entry 4320800

Structure parameters

• Formula: Cl6.5 K Os2.5 Re3.5 Se7.5
• Calculated formula: Cl6.48 K Os2.52 Re3.48 Se7.52
• Title of publication: Heterometal Substitution in the Dimensional Reduction of Cluster Frameworks: Synthesis of Soluble [Re6-nOsnSe8Cl6](4-n) (n = 1-3) Cluster-Containing Solids
• Authors of publication: Eric G. Tulsky; Jeffrey R. Long
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 6990 - 7002
• a: 12.9553 ± 0.0003 Å
• b: 12.9553 ± 0.0003 Å
• c: 12.9553 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2174.41 ± 0.09 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 201
• Hermann-Mauguin space group symbol: P n -3 :2
• Hall space group symbol: -P 2ab 2bc 3
• Residual factor for all reflections: 0.0477
• Residual factor for significantly intense reflections: 0.0224
• Weighted residual factors for all reflections: 0.0332
• Weighted residual factors for significantly intense reflections: 0.0309
• Goodness-of-fit parameter for all reflections: 0.883
• Goodness-of-fit parameter for significantly intense reflections: 0.993
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No