Information card for entry 4320803

Structure parameters

• Formula: C42 H99 Cl3 N3 Os P6 Re5 Se8
• Calculated formula: C42 H96 Cl3 N3 Os1.02 P6 Re4.98 Se8
• Title of publication: Heterometal Substitution in the Dimensional Reduction of Cluster Frameworks: Synthesis of Soluble [Re6-nOsnSe8Cl6](4-n) (n = 1-3) Cluster-Containing Solids
• Authors of publication: Eric G. Tulsky; Jeffrey R. Long
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 6990 - 7002
• a: 15.7994 ± 0.0012 Å
• b: 17.3613 ± 0.0013 Å
• c: 24.979 ± 0.002 Å
• α: 90°
• β: 97.023 ± 0.001°
• γ: 90°
• Cell volume: 6800.3 ± 0.9 ų
• Cell temperature: 165 ± 2 K
• Ambient diffraction temperature: 165 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.065
• Residual factor for significantly intense reflections: 0.0307
• Weighted residual factors for all reflections: 0.0581
• Weighted residual factors for significantly intense reflections: 0.0533
• Goodness-of-fit parameter for all reflections: 0.782
• Goodness-of-fit parameter for significantly intense reflections: 0.918
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No