Information card for entry 4320804

Structure parameters

• Formula: C36 H90 Cl0 I12 N0 O0 Os2 P6 Re4 Se8
• Calculated formula: C36 H90 I12 Os1.98 P6 Re4.02 Se8
• Title of publication: Heterometal Substitution in the Dimensional Reduction of Cluster Frameworks: Synthesis of Soluble [Re6-nOsnSe8Cl6](4-n) (n = 1-3) Cluster-Containing Solids
• Authors of publication: Eric G. Tulsky; Jeffrey R. Long
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 6990 - 7002
• a: 16.5571 ± 0.0012 Å
• b: 14.3299 ± 0.001 Å
• c: 17.3163 ± 0.0013 Å
• α: 90°
• β: 94.205 ± 0.002°
• γ: 90°
• Cell volume: 4097.4 ± 0.5 ų
• Cell temperature: 145 ± 2 K
• Ambient diffraction temperature: 145 ± 2 K
• Number of distinct elements: 10
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1254
• Residual factor for significantly intense reflections: 0.0486
• Weighted residual factors for all reflections: 0.165
• Weighted residual factors for significantly intense reflections: 0.1127
• Goodness-of-fit parameter for all reflections: 0.959
• Goodness-of-fit parameter for significantly intense reflections: 1.074
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No