Information card for entry 4321728

Structure parameters

• Formula: C76 H72 B Cl F24 O8 P2 Re2
• Calculated formula: C76 H54 B Cl F24 O8 P2 Re2
• Title of publication: Rhenium Complexes with Weakly Coordinating Solvent Ligands, cis-[Re(PR3)(CO)4(L)][BArF], L = CH2Cl2, Et2O, NC5F5: Decomposition to Chloride-Bridged Dimers in CH2Cl2 Solution
• Authors of publication: Jean Huhmann-Vincent; Brian L. Scott; Gregory J. Kubas
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 115 - 124
• a: 13.4105 ± 0.0002 Å
• b: 18.0091 ± 0.0003 Å
• c: 18.9398 ± 0.0003 Å
• α: 91.776 ± 0.001°
• β: 108.642 ± 0.001°
• γ: 103.47 ± 0.001°
• Cell volume: 4187.27 ± 0.12 ų
• Cell temperature: 193 K
• Ambient diffraction temperature: 193 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0615
• Residual factor for significantly intense reflections: 0.0525
• Weighted residual factors for all reflections: 0.1539
• Weighted residual factors for significantly intense reflections: 0.1441
• Goodness-of-fit parameter for all reflections: 1.732
• Goodness-of-fit parameter for significantly intense reflections: 1.774
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No