Information card for entry 4321729

Structure parameters

• Formula: C48 H54 Cl5 Ir N2 P2 S8 W2
• Calculated formula: C192 H216 Cl20 Ir4 N8 P8 S32 W8
• Title of publication: Syntheses and Structures of Mixed-Metal Sulfido Clusters Containing Incomplete Cubane-Type M2M'S4 and Cubane-Type M2M'2S4 Cores (M = Mo, W; M' = Rh, Ir)
• Authors of publication: Tomotake Ikada; Shigeki Kuwata; Yasushi Mizobe; Masanobu Hidai
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 64 - 69
• a: 10.521 ± 0.004 Å
• b: 32.325 ± 0.005 Å
• c: 17.277 ± 0.003 Å
• α: 90°
• β: 96.34 ± 0.02°
• γ: 90°
• Cell volume: 5840 ± 3 ų
• Cell temperature: 23 K
• Ambient diffraction temperature: 23 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.071
• Weighted residual factors for significantly intense reflections: 0.068
• Goodness-of-fit parameter for significantly intense reflections: 1.9
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No