Information card for entry 4321730

Structure parameters

• Formula: C26.5 H45 Cl3 Mo2 N2 Rh2 S8
• Calculated formula: C220 H352 Cl40 Mo16 N16 Rh16 S64
• Title of publication: Syntheses and Structures of Mixed-Metal Sulfido Clusters Containing Incomplete Cubane-Type M2M'S4 and Cubane-Type M2M'2S4 Cores (M = Mo, W; M' = Rh, Ir)
• Authors of publication: Tomotake Ikada; Shigeki Kuwata; Yasushi Mizobe; Masanobu Hidai
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 64 - 69
• a: 26.312 ± 0.004 Å
• b: 10.847 ± 0.004 Å
• c: 32.9 ± 0.003 Å
• α: 90°
• β: 111.274 ± 0.008°
• γ: 90°
• Cell volume: 8750 ± 4 ų
• Cell temperature: 23 K
• Ambient diffraction temperature: 23 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for significantly intense reflections: 0.049
• Weighted residual factors for significantly intense reflections: 0.052
• Goodness-of-fit parameter for significantly intense reflections: 4.35
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No