Information card for entry 4321950

Structure parameters

• Formula: C25.5 H23 Cl I2 P2 Pd S
• Calculated formula: C25.5 H22 Cl I2 P2 Pd S
• Title of publication: Kinetic and Mechanistic Aspects of Sulfur Recovery from Pd~2~I~2~(μ-S)(μ-dpm)~2~ Using I2 and Structures of Pd(II) Complexes with the Chelated Monosulfide of dpm
• Authors of publication: Terrance Y. H. Wong; Steven J. Rettig; Brian R. James
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2143 - 2149
• a: 9.378 ± 0.002 Å
• b: 14.231 ± 0.003 Å
• c: 21.049 ± 0.002 Å
• α: 90°
• β: 91.603 ± 0.015°
• γ: 90°
• Cell volume: 2808.1 ± 0.9 ų
• Cell temperature: 294.2 K
• Ambient diffraction temperature: 294.2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.035
• Weighted residual factors for all reflections included in the refinement: 0.028
• Goodness-of-fit parameter for all reflections included in the refinement: 1.32
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No