Information card for entry 4321951

Structure parameters

• Formula: C52 H48 Cl6 P4 Pd S2
• Calculated formula: C52 H48 Cl6 P4 Pd0.5 S2
• Title of publication: Kinetic and Mechanistic Aspects of Sulfur Recovery from Pd~2~I~2~(μ-S)(μ-dpm)~2~ Using I2 and Structures of Pd(II) Complexes with the Chelated Monosulfide of dpm
• Authors of publication: Terrance Y. H. Wong; Steven J. Rettig; Brian R. James
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2143 - 2149
• a: 11.6116 ± 0.0011 Å
• b: 11.8126 ± 0.001 Å
• c: 10.3623 ± 0.0007 Å
• α: 97.898 ± 0.006°
• β: 96.011 ± 0.007°
• γ: 80.174 ± 0.008°
• Cell volume: 1382.4 ± 0.2 ų
• Cell temperature: 294.2 K
• Ambient diffraction temperature: 294.2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.036
• Weighted residual factors for all reflections included in the refinement: 0.033
• Goodness-of-fit parameter for all reflections included in the refinement: 1.77
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No