Information card for entry 4321983

Structure parameters

• Formula: F7 K O4 Re2
• Calculated formula: F7 K O4 Re2
• SMILES: [F]([Re](F)(F)(=O)(F)=O)[Re](F)(F)(F)(=O)=O.[K+]
• Title of publication: Lewis Acid Behavior of ReO2F3: Synthesis of (ReO2F3)\ιnfty, ReO2F4-, Re2O4F7-, Re3O6F10-, and ReO2F3(CH3CN) and Study by NMR Spectroscopy, Raman Spectroscopy, and Density Functional Theory Calculations; and X-ray Structures of [Li][ReO2F4], [K][Re2O4F7], [K][Re2O4F7].2ReO2F3, [Cs][Re3O6F10], and ReO3F(CH3CN)2.CH3CN
• Authors of publication: William J. Casteel; David A. Dixon; Nicolas LeBlond; Philippa E. Lock; Hélène P. A. Mercier; Gary J. Schrobilgen
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2340 - 2358
• a: 5.499 ± 0.0011 Å
• b: 5.153 ± 0.001 Å
• c: 14.753 ± 0.003 Å
• α: 90°
• β: 95.68 ± 0.03°
• γ: 90°
• Cell volume: 415.99 ± 0.15 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.0553
• Residual factor for significantly intense reflections: 0.0473
• Weighted residual factors for all reflections: 0.1243
• Weighted residual factors for significantly intense reflections: 0.12
• Goodness-of-fit parameter for significantly intense reflections: 1.121
• Diffraction radiation wavelength: 0.56086 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No