Information card for entry 4322005

Structure parameters

• Formula: C30 H40 Br2 F6 N2 O P4 W
• Calculated formula: C120 H160 Br8 F24 N8 O4 P16 W4
• Title of publication: Synthesis and Structures of Tungsten (1-Pyridinio)imido Complexes and Their Facile N-N Bond Cleavage1
• Authors of publication: Hiroshige Ishino; Shin'ichi Tokunaga; Hidetake Seino; Youichi Ishii; Masanobu Hidai
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2489 - 2496
• a: 9.593 ± 0.001 Å
• b: 30.315 ± 0.004 Å
• c: 13.708 ± 0.002 Å
• α: 90°
• β: 108.66 ± 0.01°
• γ: 90°
• Cell volume: 3776.9 ± 0.9 ų
• Cell temperature: 23 K
• Ambient diffraction temperature: 23 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.044
• Weighted residual factors for significantly intense reflections: 0.035
• Goodness-of-fit parameter for significantly intense reflections: 1.35
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No