Information card for entry 4322006

Structure parameters

• Formula: C26 H33 Cl2 F3 N2 O4 P2 S W
• Calculated formula: C104 H132 Cl8 F12 N8 O16 P8 S4 W4
• Title of publication: Synthesis and Structures of Tungsten (1-Pyridinio)imido Complexes and Their Facile N-N Bond Cleavage1
• Authors of publication: Hiroshige Ishino; Shin'ichi Tokunaga; Hidetake Seino; Youichi Ishii; Masanobu Hidai
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2489 - 2496
• a: 8.823 ± 0.004 Å
• b: 34.939 ± 0.005 Å
• c: 10.729 ± 0.003 Å
• α: 90°
• β: 93.58 ± 0.03°
• γ: 90°
• Cell volume: 3300.9 ± 1.8 ų
• Cell temperature: 20 K
• Ambient diffraction temperature: 20 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.027
• Goodness-of-fit parameter for significantly intense reflections: 1.33
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No