Information card for entry 4322008

Structure parameters

• Formula: C17 H23 Cl2 N O P2 W
• Calculated formula: C68 H92 Cl8 N4 O4 P8 W4
• Title of publication: Synthesis and Structures of Tungsten (1-Pyridinio)imido Complexes and Their Facile N-N Bond Cleavage1
• Authors of publication: Hiroshige Ishino; Shin'ichi Tokunaga; Hidetake Seino; Youichi Ishii; Masanobu Hidai
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2489 - 2496
• a: 13.0529 ± 0.0008 Å
• b: 9.985 ± 0.002 Å
• c: 18.07 ± 0.001 Å
• α: 90°
• β: 110.755 ± 0.004°
• γ: 90°
• Cell volume: 2202.3 ± 0.5 ų
• Cell temperature: 20 K
• Ambient diffraction temperature: 20 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for significantly intense reflections: 0.027
• Weighted residual factors for significantly intense reflections: 0.018
• Goodness-of-fit parameter for significantly intense reflections: 1.55
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No