Information card for entry 4322007

Structure parameters

• Formula: C24.5 H34 Cl4 N2 O5 P2 W
• Calculated formula: C200 H280 Cl40 N16 O40 P16 W8
• Title of publication: Synthesis and Structures of Tungsten (1-Pyridinio)imido Complexes and Their Facile N-N Bond Cleavage1
• Authors of publication: Hiroshige Ishino; Shin'ichi Tokunaga; Hidetake Seino; Youichi Ishii; Masanobu Hidai
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2489 - 2496
• a: 20.266 ± 0.002 Å
• b: 10.502 ± 0.001 Å
• c: 30.363 ± 0.002 Å
• α: 90°
• β: 96.012 ± 0.007°
• γ: 90°
• Cell volume: 6426.7 ± 1 ų
• Cell temperature: 20 K
• Ambient diffraction temperature: 20 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.044
• Weighted residual factors for significantly intense reflections: 0.027
• Goodness-of-fit parameter for significantly intense reflections: 1.82
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No