Information card for entry 4322025

Structure parameters

• Formula: C299 H319 Cl3 N24 O4 Ru4 Zn
• Calculated formula: C220 H136 Cl N24 O4 Ru4 Zn
• Title of publication: Porphyrin "Flying-Saucers": Solid State and Solution Structure of a Novel Pentameric Array of Axially-Ligated Canted Porphyrins
• Authors of publication: Enzo Alessio; Silvano Geremia; Stefano Mestroni; Ivana Srnova; Miroslav Slouf; Teresa Gianferrara; Anna Prodi
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2527 - 2529
• a: 31.551 ± 0.001 Å
• b: 31.551 ± 0.001 Å
• c: 12.9 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 12841.5 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 86
• Hermann-Mauguin space group symbol: P 42/n :2
• Hall space group symbol: -P 4bc
• Residual factor for all reflections: 0.0979
• Residual factor for significantly intense reflections: 0.0832
• Weighted residual factors for significantly intense reflections: 0.237
• Weighted residual factors for all reflections included in the refinement: 0.245
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.8 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No