Information card for entry 4322027

Structure parameters

• Formula: C23 H29 Cl3 N2 O6 P2 W
• Calculated formula: C23 H29 Cl3 N2 O6 P2 W
• Title of publication: Synthesis and Structures of Tungsten (1-Pyridinio)imido Complexes and Their Facile N-N Bond Cleavage1
• Authors of publication: Hiroshige Ishino; Shin'ichi Tokunaga; Hidetake Seino; Youichi Ishii; Masanobu Hidai
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2489 - 2496
• a: 10.068 ± 0.001 Å
• b: 10.756 ± 0.001 Å
• c: 14.323 ± 0.002 Å
• α: 98.64 ± 0.01°
• β: 96.33 ± 0.009°
• γ: 96.472 ± 0.009°
• Cell volume: 1510.9 ± 0.3 ų
• Cell temperature: 293.2 K
• Ambient diffraction temperature: 293.2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.032
• Residual factor for significantly intense reflections: 0.032
• Weighted residual factors for significantly intense reflections: 0.0289
• Weighted residual factors for all reflections included in the refinement: 0.0289
• Goodness-of-fit parameter for all reflections included in the refinement: 2.014
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No