Information card for entry 4322075

Structure parameters

• Formula: C56 H69 B Ir2 N O S2
• Calculated formula: C224 H276 B4 Ir8 N4 O4 S8
• Title of publication: Preparation of Cationic Dinuclear Hydrido Complexes of Ruthenium, Rhodium, and Iridium with Bridging Thiolato Ligands and Their Reactions with Nitrosobenzene
• Authors of publication: Takafumi Iwasa; Hitoshi Shimada; Atsushi Takami; Hiroyuki Matsuzaka; Youichi Ishii; Masanobu Hidai
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2851 - 2859
• a: 11.031 ± 0.005 Å
• b: 24.316 ± 0.005 Å
• c: 19.226 ± 0.007 Å
• α: 90°
• β: 90.91 ± 0.04°
• γ: 90°
• Cell volume: 5156 ± 3 ų
• Cell temperature: 23 K
• Ambient diffraction temperature: 23 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for significantly intense reflections: 0.026
• Goodness-of-fit parameter for significantly intense reflections: 1.83
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No