Information card for entry 4322076

Structure parameters

• Formula: C58.5 H75 B Cl2 O0.5 Rh3 S2
• Calculated formula: C234 H288 B4 Cl8 O2 Rh12 S8
• Title of publication: Preparation of Cationic Dinuclear Hydrido Complexes of Ruthenium, Rhodium, and Iridium with Bridging Thiolato Ligands and Their Reactions with Nitrosobenzene
• Authors of publication: Takafumi Iwasa; Hitoshi Shimada; Atsushi Takami; Hiroyuki Matsuzaka; Youichi Ishii; Masanobu Hidai
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2851 - 2859
• a: 9.028 ± 0.0008 Å
• b: 17.032 ± 0.002 Å
• c: 37.455 ± 0.004 Å
• α: 98.453 ± 0.008°
• β: 93.899 ± 0.007°
• γ: 91.642 ± 0.008°
• Cell volume: 5679.2 ± 1 ų
• Cell temperature: 23 K
• Ambient diffraction temperature: 23 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.047
• Weighted residual factors for significantly intense reflections: 0.029
• Goodness-of-fit parameter for significantly intense reflections: 1.51
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No