Information card for entry 4322230

Structure parameters

• Formula: C56 H70 Cl8 N8 Os3
• Calculated formula: C56 H70 Cl8 N8 Os3
• SMILES: c1[n]([Os](=[N]=[Os](Cl)(=[N]=[Os]([n]2ccc(cc2)CC)([n]2ccc(cc2)CC)(Cl)(Cl)Cl)([n]2ccc(cc2)CC)([n]2ccc(cc2)CC)Cl)([n]2ccc(cc2)CC)(Cl)(Cl)Cl)ccc(c1)CC.c1(ccccc1)C.c1(ccccc1)C
• Title of publication: Electron-Rich Nitrido-Bridged Complexes. Structure and Bonding in Triosmium Dinitrido Compounds
• Authors of publication: Claire Newton; Kimberly D. Edwards; Joseph W. Ziller; Nancy M. Doherty
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 4032 - 4037
• a: 31.374 ± 0.003 Å
• b: 12.1153 ± 0.0012 Å
• c: 21.252 ± 0.002 Å
• α: 90°
• β: 130.958 ± 0.005°
• γ: 90°
• Cell volume: 6100.4 ± 1.1 ų
• Cell temperature: 158 K
• Ambient diffraction temperature: 158 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0461
• Residual factor for significantly intense reflections: 0.0274
• Weighted residual factors for all reflections: 0.058
• Weighted residual factors for significantly intense reflections: 0.052
• Goodness-of-fit parameter for all reflections: 1.031
• Goodness-of-fit parameter for significantly intense reflections: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No