Information card for entry 4322231

Structure parameters

• Formula: C70 H98 Cl12 N8 Os3
• Calculated formula: C70 H60 Cl12 N8 Os3
• Title of publication: Electron-Rich Nitrido-Bridged Complexes. Structure and Bonding in Triosmium Dinitrido Compounds
• Authors of publication: Claire Newton; Kimberly D. Edwards; Joseph W. Ziller; Nancy M. Doherty
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 4032 - 4037
• a: 17.4716 ± 0.0013 Å
• b: 17.4716 ± 0.0013 Å
• c: 26.435 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8069.5 ± 1.5 ų
• Cell temperature: 158 K
• Ambient diffraction temperature: 158 K
• Number of distinct elements: 5
• Space group number: 98
• Hermann-Mauguin space group symbol: I 41 2 2
• Hall space group symbol: I 4bw 2bw
• Residual factor for all reflections: 0.0406
• Residual factor for significantly intense reflections: 0.0325
• Weighted residual factors for all reflections: 0.085
• Weighted residual factors for significantly intense reflections: 0.0815
• Goodness-of-fit parameter for all reflections: 1.119
• Goodness-of-fit parameter for significantly intense reflections: 1.143
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No