Information card for entry 4322483

Structure parameters

• Formula: C24.5 H29 N O2.5 P Re S2
• Calculated formula: C49 H54 N2 O5 P2 Re2 S4
• Title of publication: Novel Six-Coordinate Oxorhenium "3 + 2" Mixed-Ligand Complexes Carrying the SNS/PO Donor Atom Set: Synthesis and Characterization
• Authors of publication: Berthold Nock; Theodosia Maina; Francesco Tisato; Minas Papadopoulos; Catherine P. Raptopoulou; Aris Terzis; Efstratios Chiotellis
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 4197 - 4202
• a: 16.14 ± 0.01 Å
• b: 10.384 ± 0.007 Å
• c: 15.66 ± 0.01 Å
• α: 100.11 ± 0.02°
• β: 102.71 ± 0.02°
• γ: 100.89 ± 0.02°
• Cell volume: 2449 ± 3 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0525
• Residual factor for significantly intense reflections: 0.0389
• Weighted residual factors for all reflections: 0.1011
• Weighted residual factors for significantly intense reflections: 0.0901
• Goodness-of-fit parameter for all reflections: 1.138
• Goodness-of-fit parameter for significantly intense reflections: 1.138
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No