Information card for entry 4323285

Structure parameters

• Chemical name: lithium-μ-dicyclohexylphosphido-P,P-heptacarbonyl-dirhenium-benzoylate water bis-tetrahydrofurane solvate
• Formula: C34 H46 Li O11 P Re2
• Calculated formula: C34 H43 Li O11 P Re2
• Title of publication: Stepwise Synthesis of the Functionalized Metallatetrahedron Re~2~(AuPPh~3~)~2~(μ-PCy~2~)(CO)~7~X (X = Cl, Br, I)
• Authors of publication: Hans-Jürgen Haupt; Meinhard Schwefer; Hans Egold; Ulrich Flörke
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 184 - 188
• a: 10.536 ± 0.002 Å
• b: 11.433 ± 0.002 Å
• c: 19.125 ± 0.003 Å
• α: 98.01 ± 0.01°
• β: 89.94 ± 0.01°
• γ: 112.22 ± 0.01°
• Cell volume: 2108.5 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0912
• Residual factor for significantly intense reflections: 0.0537
• Weighted residual factors for all reflections: 0.1705
• Weighted residual factors for significantly intense reflections: 0.1401
• Goodness-of-fit parameter for all reflections: 1.054
• Goodness-of-fit parameter for significantly intense reflections: 1.071
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No