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Information card for entry 4323286
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Jmol._Canvas2D (Jmol) "jmolApplet0"[x]
Coordinates | 4323286.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | μ-dicyclohexylphosphido-P,P-bis(triphenylphosphido-gold)- chloro-heptacarbonyl-dirhenium dichloromethane solvate |
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Formula | C56 H54 Au2 Cl3 O7 P3 Re2 |
Calculated formula | C56 H54 Au2 Cl3 O7 P3 Re2 |
SMILES | [Au]12([Au]3([Re]41([Re]23([P]4(C1CCCCC1)C1CCCCC1)(C#[O])(C#[O])(C#[O])C#[O])(Cl)(C#[O])(C#[O])C#[O])[P](c1ccccc1)(c1ccccc1)c1ccccc1)[P](c1ccccc1)(c1ccccc1)c1ccccc1.C(Cl)Cl |
Title of publication | Stepwise Synthesis of the Functionalized Metallatetrahedron Re~2~(AuPPh~3~)~2~(μ-PCy~2~)(CO)~7~X (X = Cl, Br, I) |
Authors of publication | Hans-Jürgen Haupt; Meinhard Schwefer; Hans Egold; Ulrich Flörke |
Journal of publication | Inorganic Chemistry |
Year of publication | 1997 |
Journal volume | 36 |
Pages of publication | 184 - 188 |
a | 18.615 ± 0.005 Å |
b | 13.606 ± 0.002 Å |
c | 24.223 ± 0.006 Å |
α | 90° |
β | 105.14 ± 0.02° |
γ | 90° |
Cell volume | 5922 ± 2 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1936 |
Residual factor for significantly intense reflections | 0.0744 |
Weighted residual factors for all reflections | 0.1596 |
Weighted residual factors for significantly intense reflections | 0.1194 |
Goodness-of-fit parameter for all reflections | 0.97 |
Goodness-of-fit parameter for significantly intense reflections | 1.111 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4323286.html
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