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Information card for entry 4323316
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Jmol._Canvas2D (Jmol) "jmolApplet0"[x]
Coordinates | 4323316.cif |
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Original paper (by DOI) | HTML |
Common name | cis-Tetrachloro-bis(dihexylamido)-bis(diethylphosphine)ditungsten(III) |
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Chemical name | 1,1,2,2-Tetrachloro-1,2-bis(dihexylamido)-(cis)- 1,2-bis(diethylphosphine)ditungsten(III) |
Formula | C32 H74 Cl4 N2 P2 W2 |
Calculated formula | C32 H74 Cl4 N2 P2 W2 |
Title of publication | W2Cl4(NR2)2(PR'3)2 Molecules. 4. A New Synthetic Route to Products with a Staggered Conformation. Preparations and Characterizations of W2Cl4(NR2)2(PR'3)2 (R = Et, Bu, Hex; R'3= Me3, Et2H) and an Intermediate Complex W2Cl4(NEt2)2(NHEt2)2 |
Authors of publication | F. Albert Cotton; Evgeny V. Dikarev; N. Nawar; Wai-Yeung Wong |
Journal of publication | Inorganic Chemistry |
Year of publication | 1997 |
Journal volume | 36 |
Pages of publication | 559 - 566 |
a | 15.3937 ± 0.0007 Å |
b | 11.473 ± 0.002 Å |
c | 24.977 ± 0.003 Å |
α | 90° |
β | 92.33 ± 0.01° |
γ | 90° |
Cell volume | 4407.6 ± 1 Å3 |
Cell temperature | 213 ± 2 K |
Ambient diffraction temperature | 213 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0546 |
Residual factor for significantly intense reflections | 0.0435 |
Weighted residual factors for all reflections | 0.105 |
Weighted residual factors for significantly intense reflections | 0.0995 |
Goodness-of-fit parameter for all reflections | 1.087 |
Goodness-of-fit parameter for significantly intense reflections | 1.12 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4323316.html
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