Information card for entry 4323507

Structure parameters

• Formula: C39 H32 Cl2 N P2 Rh
• Calculated formula: C39 H32 Cl2 N P2 Rh
• Title of publication: A Bidentate Bisphosphine Functioning in Intramolecular Aliphatic Metalation and as an NMR Spectroscopic Probe for the Metal Coordination Environment
• Authors of publication: William Lesueur; Euro Solari; Carlo Floriani; Angiola Chiesi-Villa; Corrado Rizzoli
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 3354 - 3362
• a: 15.346 ± 0.002 Å
• b: 18.188 ± 0.003 Å
• c: 12.072 ± 0.002 Å
• α: 90 ± 0°
• β: 90 ± 0°
• γ: 90 ± 0°
• Cell volume: 3369.5 ± 0.9 ų
• Cell temperature: 25 K
• Ambient diffraction temperature: 295 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1009
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for all reflections: 0.1665
• Weighted residual factors for significantly intense reflections: 0.1139
• Goodness-of-fit parameter for all reflections: 0.852
• Goodness-of-fit parameter for significantly intense reflections: 0.938
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No