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Information card for entry 4323508
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Coordinates | 4323508.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C39 H34 Cl6 P2 Pd |
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Calculated formula | C41 H32 Cl10 P2 Pd |
Title of publication | A Bidentate Bisphosphine Functioning in Intramolecular Aliphatic Metalation and as an NMR Spectroscopic Probe for the Metal Coordination Environment |
Authors of publication | William Lesueur; Euro Solari; Carlo Floriani; Angiola Chiesi-Villa; Corrado Rizzoli |
Journal of publication | Inorganic Chemistry |
Year of publication | 1997 |
Journal volume | 36 |
Pages of publication | 3354 - 3362 |
a | 11.987 ± 0.001 Å |
b | 15.99 ± 0.002 Å |
c | 10.872 ± 0.001 Å |
α | 91.42 ± 0.01° |
β | 111.01 ± 0.02° |
γ | 99.86 ± 0.02° |
Cell volume | 1908.2 ± 0.5 Å3 |
Cell temperature | 25 K |
Ambient diffraction temperature | 298 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0537 |
Residual factor for significantly intense reflections | 0.0526 |
Weighted residual factors for all reflections | 0.1519 |
Weighted residual factors for significantly intense reflections | 0.1427 |
Goodness-of-fit parameter for all reflections | 1.102 |
Goodness-of-fit parameter for significantly intense reflections | 1.034 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4323508.html
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