Information card for entry 4323533

Structure parameters

• Formula: C17 H27 F12 N8 O2 P2 Re
• Calculated formula: C17 H24 F12 N8 O2 P2 Re
• Title of publication: Oxo Ligand Reactivity in the [ReO2L4]+ Complex of 1-Methylimidazole. Preparation and Crystal Structures of Salts Containing the ReOL43+ Core and Apical CH3O-, BF3O2-, and (CH3O)2PO2- Groups
• Authors of publication: Suzanne Bélanger; André L. Beauchamp
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 3640 - 3647
• a: 13.022 ± 0.003 Å
• b: 13.022 Å
• c: 17.218 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2919.7 ± 1.1 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 7
• Space group number: 130
• Hermann-Mauguin space group symbol: P 4/n c c :2
• Hall space group symbol: -P 4a 2ac
• Residual factor for all reflections: 0.0428
• Residual factor for significantly intense reflections: 0.0271
• Weighted residual factors for all reflections: 0.0758
• Weighted residual factors for significantly intense reflections: 0.0698
• Goodness-of-fit parameter for all reflections: 0.916
• Goodness-of-fit parameter for significantly intense reflections: 1.027
• Diffraction radiation wavelength: 1.54056 Å
• Diffraction radiation type: CopperKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No